Full Report Set



  ASAP 2020 V3.01 H    Unit 1    Serial #: 220    Page  1  

     Sample:    SJO-1413                          
   Operator:                                      
  Submitter:                                      
       File:    C:\2020\DATA\DUMELE\SJO-1413.SMP  

            Started:    18.11.2021 9:30:19        Analysis Adsorptive:    N2                    
          Completed:    21.11.2021 23:17:37       Analysis Bath Temp.:    -195.650 C           
        Report Time:    24.11.2021 9:34:36         Thermal Correction:    No                    
        Sample Mass:    0.0447 g                      Warm Free Space:    15.9268 cm Measured  
    Cold Free Space:    48.6978 cm            Equilibration Interval:    45 s                  
  Low Pressure Dose:    0.5000 mmol/g                 Automatic Degas:    No                    







                      Isotherm Tabular Report

   Relative       Absolute      Quantity    Elapsed    Saturation   
   Pressure       Pressure      Adsorbed     Time       Pressure    
    (p/p)         (mbar)       (mmol/g)    (h:min)      (mbar)     
-----
  1.#QNAN0000       1.#QNAN0     1.#QNAN      00:58    1033.328672  
  0.000010672       0.011027     0.51207      01:54       1.#QNAN0  
  0.000010247       0.010588     1.02413      02:43       1.#QNAN0  
  0.000027462       0.028375     1.53084      03:37       1.#QNAN0  
  0.000064622       0.066770     2.02691      05:41       1.#QNAN0  
  0.000137432       0.141989     2.50277      09:24       1.#QNAN0  
  0.000266191       0.274992     2.94146      13:56       1.#QNAN0  
  0.000451162       0.466037     3.32588      18:28       1.#QNAN0  
  0.000895602       0.925065     3.81634      21:59       1.#QNAN0  
  0.001631418       1.684989     4.28907      24:53       1.#QNAN0  
  0.002801075       2.892911     4.74846      27:23       1.#QNAN0  
  0.004488579       4.635495     5.18312      30:03       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      30:14    1032.727321  
  0.007074322       7.304622     5.58820      30:29       1.#QNAN0  
  0.010349838      10.685577     5.94576      30:39       1.#QNAN0  
  0.011740100      12.120261     6.07661      30:44       1.#QNAN0  
  0.012223180      12.618421     6.12076      30:48       1.#QNAN0  
  0.013351590      13.782702     6.21127      30:52       1.#QNAN0  
  0.014115856      14.570670     6.27527      30:58       1.#QNAN0  
  0.016128247      16.646227     6.42623      31:07       1.#QNAN0  
  0.017143636      17.693040     6.49789      31:13       1.#QNAN0  
  0.018356012      18.943423     6.57791      31:17       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      31:22    1031.943368  
  0.020810483      21.473428     6.73236      31:28       1.#QNAN0  
  0.023846891      24.604834     6.89629      31:33       1.#QNAN0  
  0.026858473      27.709797     7.04773      31:39       1.#QNAN0  
  0.030287809      31.244755     7.20974      31:46       1.#QNAN0  
  0.033785535      34.850541     7.36013      31:51       1.#QNAN0  
  0.034632555      35.722753     7.39696      31:54       1.#QNAN0  
  0.040009344      41.265895     7.59864      31:59       1.#QNAN0  
  0.044943426      46.351678     7.77222      32:04       1.#QNAN0  
  0.051376425      52.981775     7.97835      32:10       1.#QNAN0  
  0.052113071      53.739169     8.01204      32:13       1.#QNAN0  
  0.052444132      54.078278     8.02553      32:16       1.#QNAN0  
  0.053891717      55.567841     8.07103      32:20       1.#QNAN0  
  0.054382827      56.072647     8.08587      32:22       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      32:25    1031.029137  
  0.055226985      56.941543     8.12322      32:29       1.#QNAN0  
  0.057135900      58.910666     8.17977      32:33       1.#QNAN0  
  0.058388762      60.203167     8.21702      32:36       1.#QNAN0  
  0.059839417      61.699642     8.25835      32:39       1.#QNAN0  
  0.061410290      63.320364     8.30357      32:43       1.#QNAN0  
  0.063424029      65.397784     8.35511      32:47       1.#QNAN0  
  0.065083689      67.110168     8.39986      32:51       1.#QNAN0  
  0.067049765      69.138292     8.45154      32:54       1.#QNAN0  
  0.068910522      71.057863     8.49931      32:57       1.#QNAN0  
  0.071017474      73.231350     8.55090      33:00       1.#QNAN0  
  0.073216212      75.499841     8.60226      33:04       1.#QNAN0  
  0.075461705      77.816306     8.65475      33:07       1.#QNAN0  
  0.080112568      82.613612     8.75521      33:11       1.#QNAN0  
  0.085888546      88.571329     8.87286      33:15       1.#QNAN0  
  0.097365514     100.408799     9.08464      33:20       1.#QNAN0  
  0.100066686     103.195639     9.13154      33:23       1.#QNAN0  
  0.111242062     114.722292     9.31636      33:27       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      33:30    1031.297588  
  0.126637692     130.595919     9.55652      33:34       1.#QNAN0  
  0.140534966     144.921770     9.76080      33:38       1.#QNAN0  
  0.143632880     148.111938     9.81240      33:41       1.#QNAN0  
  0.163999043     169.106432    10.08750      33:45       1.#QNAN0  
  0.187269933     193.092380    10.34814      33:50       1.#QNAN0  
  0.213995433     220.642184    10.56550      33:53       1.#QNAN0  
  0.243276762     250.822957    10.76708      33:57       1.#QNAN0  
  0.252468827     260.292334    10.84928      34:00       1.#QNAN0  
  0.276090161     284.637099    11.00039      34:03       1.#QNAN0  
  0.301472159     310.795517    11.13717      34:06       1.#QNAN0  
  0.314072753     323.779315    11.20599      34:08       1.#QNAN0  
  0.350714008     361.542128    11.38150      34:11       1.#QNAN0  
  0.373393154     384.909922    11.49033      34:14       1.#QNAN0  
  0.400573798     412.920646    11.61865      34:16       1.#QNAN0  
  0.404380803     416.832475    11.64932      34:19       1.#QNAN0  
  0.450480903     464.338142    11.84745      34:22       1.#QNAN0  
  0.478045514     492.740801    11.97399      34:24       1.#QNAN0  
  0.500584433     515.957078    12.07875      34:27       1.#QNAN0  
  0.523877197     539.954337    12.18802      34:29       1.#QNAN0  
  0.550586564     567.472018    12.31881      34:31       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      34:34    1030.637161  
  0.595917265     614.187507    12.54022      34:37       1.#QNAN0  
  0.600062926     618.469016    12.58252      34:39       1.#QNAN0  
  0.650951908     670.933179    12.83866      34:42       1.#QNAN0  
  0.693928451     715.244080    13.08716      34:45       1.#QNAN0  
  0.700358788     721.887252    13.14983      34:48       1.#QNAN0  
  0.741238995     764.040290    13.42044      34:51       1.#QNAN0  
  0.772110440     795.878255    13.67083      34:54       1.#QNAN0  
  0.807609010     832.487232    14.01287      34:57       1.#QNAN0  
  0.871238734     898.108803    14.88404      35:02       1.#QNAN0  
  0.912860855     941.061173    15.93522      35:09       1.#QNAN0  
  0.927265142     955.944230    16.50353      35:14       1.#QNAN0  
  0.945983370     975.289649    17.61973      35:21       1.#QNAN0  
  0.953880264     983.472897    18.28916      35:27       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      35:38    1031.103594  
  0.982723552    1013.327626    24.26873      35:48       1.#QNAN0  
  0.994402577    1025.423965    29.07175      36:02       1.#QNAN0  
  0.982033835    1012.688274    27.98426      36:07       1.#QNAN0  
  0.975041503    1005.507711    26.41006      36:15       1.#QNAN0  
  0.969798857    1000.134860    25.04574      36:24       1.#QNAN0  
  0.967183967     997.460519    24.42290      36:30       1.#QNAN0  
  0.964099018     994.301273    23.67788      36:36       1.#QNAN0  
  0.959107971     989.187109    22.55453      36:45       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      36:47    1031.369278  
  0.952332320     982.215025    21.29167      36:55       1.#QNAN0  
  0.947622378     977.365976    20.51718      37:03       1.#QNAN0  
  0.939672558     969.175241    19.48216      37:11       1.#QNAN0  
  0.933544999     962.861713    18.85705      37:17       1.#QNAN0  
  0.925863043     954.945939    18.16078      37:24       1.#QNAN0  
  0.913975488     942.692306    17.40516      37:31       1.#QNAN0  
  0.906787704     935.282838    17.00021      37:35       1.#QNAN0  
  0.889023927     916.966957    16.28922      37:41       1.#QNAN0  
  0.876421375     903.973313    15.90422      37:46       1.#QNAN0  
  0.860822224     887.887718    15.51275      37:50       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      37:52    1031.443735  
  0.840151884     866.578186    15.10557      37:56       1.#QNAN0  
  0.820476326     846.292333    14.80682      38:00       1.#QNAN0  
  0.800650703     825.849186    14.55069      38:03       1.#QNAN0  
  0.770209640     794.458124    14.22572      38:07       1.#QNAN0  
  0.740339467     763.653358    13.96427      38:10       1.#QNAN0  
  0.700404504     722.466306    13.67690      38:13       1.#QNAN0  
  0.650556926     671.055402    13.36590      38:17       1.#QNAN0  
  0.600348921     619.270098    13.09581      38:20       1.#QNAN0  
  0.550330299     567.679358    12.85634      38:23       1.#QNAN0  
  0.500389193     516.167794    12.63095      38:26       1.#QNAN0  
  0.451542356     465.785411    12.30839      38:30       1.#QNAN0  
  0.398116700     410.677666    12.06806      38:33       1.#QNAN0  
  0.351425359     362.515926    11.86135      38:36       1.#QNAN0  
  0.300350820     309.831892    11.62316      38:39       1.#QNAN0  
  0.250672763     258.588942    11.34447      38:44       1.#QNAN0  
  0.200565307     206.901205    10.99736      38:48       1.#QNAN0  
  0.152009723     156.814126    10.45158      38:54       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      38:56    1031.611120  
  0.100360719     103.532617     9.65693      39:03       1.#QNAN0  
  0.069718148      71.921160     9.02865      39:10       1.#QNAN0  




  ASAP 2020 V3.01 H    Unit 1    Serial #: 220    Page  1  

     Sample:    SJO-1413                          
   Operator:                                      
  Submitter:                                      
       File:    C:\2020\DATA\DUMELE\SJO-1413.SMP  

            Started:    18.11.2021 9:30:19        Analysis Adsorptive:    N2                    
          Completed:    21.11.2021 23:17:37       Analysis Bath Temp.:    -195.650 C           
        Report Time:    24.11.2021 9:34:36         Thermal Correction:    No                    
        Sample Mass:    0.0447 g                      Warm Free Space:    15.9268 cm Measured  
    Cold Free Space:    48.6978 cm            Equilibration Interval:    45 s                  
  Low Pressure Dose:    0.5000 mmol/g                 Automatic Degas:    No                    







 Options Report


              Sample Tube

         Warm freespace:    1.0000 cm  
         Cold freespace:    1.0000 cm  
    Non-ideality factor:    0.0000620   
  Use Isothermal Jacket:    Yes         
         Use Filler Rod:    Yes         
       Vacuum seal type:    Seal Frit   

 Analysis Conditions


                 Preparation

               Fast evacuation:    No        
  Unrestricted evacuation from:    6.7 mbar  
               Vacuum setpoint:    13 bar   
               Evacuation time:    0.10 h    
                     Leak test:    No        
                 Use TransSeal:    No        

                Free Space

             Free-space type:    Measured  
  Lower dewar for evacuation:    Yes       
             Evacuation time:    0.10 h    
                 Outgas test:    No        

                                                       p and Temperature

         p and T type:    Measure p at intervals during analysis.  Calculate the Analysis Bath Temperature from these values.  
  Measurement interval:    60 min                                                                                                

                         Dosing

  Use first pressure fixed dose:    No                  
   Use maximum volume increment:    No                  
               Target tolerance:    5.0% or 6.666 mbar  
            Low pressure dosing:    Yes                 
                    Dose amount:    0.50000 mmol/g      
    Minimum equilibration delay:    0.00 h              
    Maximum equilibration delay:    999.00 h            

                      Equilibration

       Equilibration time (p/p = 0.010000000):    45 s   
       Equilibration time (p/p = 1.000000000):    10 s   
  Minimum equilibration delay at p/p >= 0.995:    600 s  

             Sample Backfill

  Backfill at start of analysis:    Yes  
    Backfill at end of analysis:    Yes  
                   Backfill gas:    N2   

                Adsorptive Properties

                         Adsorptive:    Nitrogen      
          Maximum manifold pressure:    1233.23 mbar  
                Non-ideality factor:    0.0000620     
          Density conversion factor:    0.0015468     
  Therm. tran. hard-sphere diameter:    0.386 nm      
     Molecular cross-sectional area:    0.162 nm     


  Inside diameter of sample tube:    9.53 mm  

